滕州市浩瀚色譜儀器技術(shù)服務(wù)有限公司，建立同時測定食品包裝材料中32種揮發(fā)性有機(jī)化合物（VOCs）的氣相色譜-質(zhì)譜檢測方法。方法 設(shè)定平衡溫度和時間分別為100 ℃和30 min，色譜柱為HP-VOC，載氣為氦氣，流速為2.0 mL/min，不分流進(jìn)樣，進(jìn)樣口溫度為250 ℃，柱溫為程序升溫。定量分析采用外標(biāo)法。結(jié)果 方法檢出限在0.01～0.17 mg/m2的范圍內(nèi)，相關(guān)系數(shù)＞0.99，樣品加標(biāo)回收率為90.3%～109.9%，相對標(biāo)準(zhǔn)偏差為1.1%～8.9%（n=6）。結(jié)論 該方法適用于食品包裝材料中揮發(fā)性有機(jī)化合物的測試。

包裝材料揮發(fā)性有機(jī)物VOCs測定 圖片：




Determination of volatile organic compounds VOCs in packaging materials
Determination of volatile organic compounds VOCs in packaging materials

Stationary phase: polyethylene glycol
Specification: 60m*0.32mm*0.25um
Model: HH-INNOWAX
Application: SNT 4148-2015 Determination of Volatile Organic Compounds (VOCs) in Packaging Materials - Static Headspace - Gas Chromatography
Tengzhou Haohao Chromatography Instrument Technology Service Co., Ltd. established a gas chromatography-mass spectrometry method for simultaneous determination of 32 volatile organic compounds (VOCs) in food packaging materials. The method was to set the equilibrium temperature and time to 100 °C and 30 min respectively. The column was HP-VOC, the carrier gas was helium, the flow rate was 2.0 mL/min, and the split-flow injection was performed. The inlet temperature was 250 °C. For programming. Quantitative analysis was performed using an external standard method. Results The detection limit of the method was in the range of 0.01～0.17 mg/m2, the correlation coefficient was >0.99, the recoveries of the samples were 90.3%～109.9%, and the relative standard deviations were 1.1%～8.9% (n=6). Conclusion This method is suitable for the testing of volatile organic compounds in food packaging materials.

Determination of volatile organic compounds VOCs in packaging materials